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http://hdl.handle.net/20.500.12358/26165
TitleSynthesis and structure of 2-aryl-5, 5-disubstituted-1, 3-dioxanes and conversion into chiral (1, 1, 1-trishydroxymethyl) methane derivatives
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Abstract

Pentaerythritol, (1,1,1-trishydroxymethyl)methyl methane and (1,1,1-trishydroxymethyl)nitromethane are converted into 2-aryl-5,5-bis(hydroxymethyl), 2-aryl-5-hydroxymethyl-5-methyl- or 2-aryl-5-hydroxymethyl-5-nitro-1,3-dioxanes and a range of derivatives. X-Ray and NMR analysis establishes that the latter is obtained as a single diastereomer whose structure is unambiguously determined. These materials can be elaborated to chiral derivatives of the starting (1,1,1-trishydroxymethyl) methanes.

Authors
Gardiner, John M
Mather, Paul
Morjan, Ramy Y.
Pritchard, Robin G
Warren, John E
Cooper, Malcolm L
Ferwanah, Abdel-Rahman S.
Abu-Tiem, Omar S
TypeJournal Article
Date2002
Published inTetrahedron letters
SeriesVolume: 43, Number: 11
PublisherPergamon
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The institutional repository of the Islamic University of Gaza was established as part of the ROMOR project that has been co-funded with support from the European Commission under the ERASMUS + European programme. This publication reflects the views only of the author, and the Commission cannot be held responsible for any use which may be made of the information contained therein.

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The institutional repository of the Islamic University of Gaza was established as part of the ROMOR project that has been co-funded with support from the European Commission under the ERASMUS + European programme. This publication reflects the views only of the author, and the Commission cannot be held responsible for any use which may be made of the information contained therein.

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